Electrical Engineering

Research > Faculty Projects

Development of a MEMS-based Ultra-high Temperature Heating Element for the TEM

Principal Investigator
Karl F. Bohringer

Sponsor(s)
Washington Technology Center (WTC)

Award Period
07/01/2007 - 04/01/2008

Abstract
Dynamic electron microscopy experiments allow direct correlations to be made between materials processing conditions, microstructure, properties and performance. This approach not only permits deeper understanding of the basic physical processes involved, but also allows rapid exploration of a matrix of conditions and effects. Perhaps the most common dynamic microscopy experiments revolve around the relatively simple act of heating a sample, as temperature is often the primary thermodynamic driving force for microstructural change in materials processing. However, the current state of the art in heating and cooling holder design relies on substantially out-dated technologies, yielding significant problems with respect to overall temperature range, drift/stability issues, expensive and time consuming maintenance and lack of precise and simple temperature control. In this proposal, our goal is to develop precision control of specimen temperature (to an accuracy of 10oC in the range 5-2000K) in response to the need for dramatically improved instrumentation in this area. This is in fact an ambitious goal, requiring substantial changes in methodology, materials selection and thermal design. Continuing progress from Phase I, the Phase II proposal will expand to address advanced methods of highly accurate temperature sensing in- situ at ultra-high temperatures (2000K) for the TEM.

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